Lab Report: Separation and Purification of Organic Compounds: Crystallization

Topics: Crystallization, Chemistry, Solution Pages: 3 (776 words) Published: August 14, 2013
Colegio de San Juan de Letran
College of Liberal Arts and Sciences

Experiment #3

Gomez, Paola Anne M. DOP: 2 July 2013
Student no. : 4120403DOS: 9 July 2013
Group: Carcinogenic

Remarks: _____________________________________________________________________

Engr. C. D. Sanchez


Crystallization is a technique which chemists use to purify solid compounds. It is one of the fundamental procedures each chemist must master to become proficient in the laboratory. Crystallization is based on the principles of solubility: compounds (solutes) tend to be more soluble in hot liquids (solvents) than they are in cold liquids. If a saturated hot solution is allowed to cool, the solute is no longer soluble in the solvent and forms crystals of pure compound. Impurities are excluded from the growing crystals and the pure solid crystals can be separated from the dissolved impurities by filtration. (

A desirable solvent for crystallization has the following properties: 1) dissolves the solute readily at an elevated temperature, but only sparingly at a lower temperature (room temperature); 2) gives no chemical reaction with the solute; and 3) is sufficiently volatile so that it may be removed easily from the purified crystals.

The crystallization process consists of two major events, nucleation and crystal growth. Nucleation is the step where the solute molecules dispersed in the solvent start to gather into clusters, on the nanometer scale (elevating solute concentration in a small region), that become stable under the current operating conditions. These stable clusters constitute the nuclei. However, when the clusters are not stable, they redissolve. Therefore, the clusters need to reach a critical size in order to become stable nuclei. Such critical size is dictated by the operating conditions (temperature,...
Continue Reading

Please join StudyMode to read the full document

You May Also Find These Documents Helpful

  • Essay about The Separation and Purification of Organic Compounds
  • sample lab reoort on purification and separation of organic compounds Essay
  • Separation and Purification of Organic Compounds Research Paper
  • Essay about Separation of Organic Liquids Report
  • Organic Compounds Lab Report Essay
  • Organic Lab Report Essay
  • Essay about Organic 2 Lab Report- Aldehydes & Ketones: Finding an Unknown
  • Lab Report for Experiment #2: Purification of Acetanilide by Recrystallization Essay

Become a StudyMode Member

Sign Up - It's Free
Fairy Tail 421 | Boku no Hero Academia | 7×03 Una Lezione Per Mike